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複合非破壞試驗法을 利用한 現場콘크리트 强度推定에 關한 硏究
조철희,김하진,이승엽,김정섭 朝鮮大學校 建設技術硏究所 1999 建設技術硏究 Vol.19 No.1
This study is to improve the reliability of compressive strength estimation using combined non-destructive testing method in estimating the compressive strength of in-situ concrete after 730 days of age, measures the values of compressive strength and non-destructive test of in-situ concrete with the combined strength of 240kg/㎠, conducts the experiment for estimating the compressive strength, makes the estimation expression of the results through simple and duplicate regressive analysis and then the results of comparing and analyzing to existing expressions to secure the range of application of estimation expression and its reliability are as follows. It is found that the positive curing is very important in the early curing of the strength revelation in long-term age and especially in hydrate and it is considered that the formation and application of estimation expression of comprressive strength according to placement and curing method are needed to enhance the degree of strength estimation of in-situ concrete. After 365 days of age, the compressive strength of concrete tends to be decreased. While the single method has not a great change of non-destructive test value according to the change of concrete strength, the combined method shows a high reliability and then it is appropriate to use it for the exact strength estimation. Existing estimation expression used for estimating the compressive strength indicates a high estimation error in comparison with the expression suggested by this research in the difference of materials used, combined strength of concrete and the difference of placement and curing methods. Accordingly, it will be desirable to use an estimation expression suitable to the in-situ conditions for the exact strength estimation. The estimation expression of compressive strength using combined non-destructive test method of in-situ concrete on 730 days of age (2 years) suggested by this research is as follows. Air Curing fc' = 7.33R+219Vp-846 [R-sq(adj) = 0.839, N=81] Water Curing fc' = 12.6R+176Vp-805 [R-sq(adj) = 0.839, N=81]
포도 송이가지를 이용한 레스베라트롤의 추출 및 항산화 활성
조철희,김소영,유귀재,손민희,박근형,임병락,김동청,채희정 한국응용생명화학회 2008 Journal of Applied Biological Chemistry (J. Appl. Vol.51 No.1
The extraction conditions for resveratrol production from grape fruit stem, which is a by-product of grape processing, were optimized to develop high-functional grape-based products. Additionally, the bioefficacy of grape fruit stem extract (GFSE) as an antioxidant agent was evaluated. Resveratrol was extracted using various experimental conditions such as extractant type, extractant concentration, raw material-extractant ratio, extraction time and temperature, and the results were analyzed using a statistical program (SPSS). The resveratrol yield was the highest when 80% ethanol with a raw-material-extractant ratio of 1 : 10 (w/v) was used. In addition, the optimal temperature and time were selected as 60oC and 90 min, respectively. When the antioxidant activity was analyzed and expressed as DPPH radical scavenging activity and SOD-like activity, the antioxidant activity of GFSE was higher than that of BHT, BHA and L-ascorbic acid. Finally, it was found that GFSE could be used as a raw material for the production of high antioxidant agents. The extraction conditions for resveratrol production from grape fruit stem, which is a by-product of grape processing, were optimized to develop high-functional grape-based products. Additionally, the bioefficacy of grape fruit stem extract (GFSE) as an antioxidant agent was evaluated. Resveratrol was extracted using various experimental conditions such as extractant type, extractant concentration, raw material-extractant ratio, extraction time and temperature, and the results were analyzed using a statistical program (SPSS). The resveratrol yield was the highest when 80% ethanol with a raw-material-extractant ratio of 1 : 10 (w/v) was used. In addition, the optimal temperature and time were selected as 60oC and 90 min, respectively. When the antioxidant activity was analyzed and expressed as DPPH radical scavenging activity and SOD-like activity, the antioxidant activity of GFSE was higher than that of BHT, BHA and L-ascorbic acid. Finally, it was found that GFSE could be used as a raw material for the production of high antioxidant agents.
조철희 한국막학회 2016 한국막학회 총회 및 학술발표회 Vol.2016 No.05
제올라이트 분리막은 알루미나 등 다공성 지지체 표면에 3차원적으로 서로 연결된 주기적인 미세기공을 갖는 제올라이트 층을 치밀하게 코팅한 복합 소재 이다. 현재 LTA, FAU, CHA, MOR, DDR 제올라이트 분리막이 투과증발 분야에서 상업화되었고 이는 PVA 판형 막에 비하여 현저한 물 투과도와 물/알코올 선택도를 갖기 때문이다. 국내의 경우도 충남대와 (주)파인텍 연구팀이 성공적으로 LTA, CHA 제올라이트 분리막을 연구하고 그 막모듈과 시스템을 상용화하였다. 본 발표에서는 국내외 제올라이트 분리막 개발 및 응용 동향을 소개하고, 특히 제올라이트 분리막이 투과증발 및 증기투과 분야에서 적용할 수 있는 유망 분야에 대하여 논의하도록 한다.