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申東秀 계명대학교 산업기술연구소 1992 産業技術硏究所 論文報告集 Vol.15 No.2
Spouted beds and fluidized beds were compared as equipments for rice hull combustion as a means of getting cheap and safe energy from agricultural wastes. The minimum and incipient spouting velocities were compared with the minimum fluidizing velocities: the maximum pressure drops were compared between the spouted and fluidized beds. The optimum operating conditions to urn rice hulls in spouted and fluidized beds were also observed
신동수,박두천,주우홍,김형국 國立 昌原大學校 基礎科學硏究所 1994 基礎科學硏究所論文集 Vol.6 No.-
O-(tert-Butyldiphenylsily1)-cis-5-methyl-4-hepten-6-yn-1-ol, an intermediate in the synthesis of taxol, was efficiently synthesized from 3-methyl-2-penten-4-yn-1-ol by sequential alcohol/bromide interchange [NBS, PPh_(3), CH_(2)Cl_(2), -30℃, 82%], displacement with the lithium salt of tert-butylacetate [LDA, THF, -78 to 23℃, 84%], LAH reduction, and silylation [tBuPhSiCl, imidazole, CH_(2)Cl_(2), 45℃, 88%].
α-위치에 작용기를 가지는 Benzylamine의 합성
김흥재,감경희,조수동,안철진,이영근,신동수 Institute of Genetic Engineering Changwon National 1999 Gene and Protein Vol.3 No.1
We have investigated the first synthetic methodology of phthalimide-benzylacetate from benzylphthalimide which are easily prepared to phthalimide as starting material. Phthalimide-benzylacetate was afforded in NBS, sodium acetate, acetic acid and chlorobenzene condition as good yield. Finally, amino(phenyl)methyl acetate(1) was synthesized from phthalimide-benzylacetate under hydrazine monohydrate, acetic acid.