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Kouhkan, Mehri,Zeynizadeh, Behzad Korean Chemical Society 2011 Bulletin of the Korean Chemical Society Vol.32 No.9
Various aldoximes and ketoximes were efficiently reduced to their corresponding amines with $NaBH_3CN$ in the presence of $MoCl_5/NaHSO_4{\cdot}H_2O$ system. Reduction reactions were carried out in refluxing EtOH or DMF within 0.3-3.8 h to afford the amines in high to excellent yields.
Kouhkan, Mehri,Zeynizadeh, Behzad Korean Chemical Society 2010 Bulletin of the Korean Chemical Society Vol.31 No.10
Reduction of carbonyl compounds such as aldehydes, ketones, $\alpha,\beta$-unsaturated enals and enones, $\alpha$-diketones and acyloins was carried out readily with $NaBH_3CN$ in the presence of wet $SiO_2$ as a neutral media. The reactions were performed at solvent-free conditions in oil bath (70 - $80^{\circ}C$) or under microwave irradiation (240 W) to give the product alcohols in high to excellent yields. Regioselective 1,2-reduction of conjugated carbonyl compounds took place in a perfect selectivity without any side product formation.
Mehri Kouhkan,Behzad Zeynizadeh 대한화학회 2010 Bulletin of the Korean Chemical Society Vol.31 No.10
Reduction of carbonyl compounds such as aldehydes, ketones, α,β-unsaturated enals and enones, α-diketones and acyloins was carried out readily with NaBH3CN in the presence of wet SiO2 as a neutral media. The reactions were performed at solvent-free conditions in oil bath (70 - 80 oC) or under microwave irradiation (240 W) to give the product alcohols in high to excellent yields. Regioselective 1,2-reduction of conjugated carbonyl compounds took place in a perfect selectivity without any side product formation.
Mehri Kouhkan,Behzad Zeynizadeh 대한화학회 2011 Bulletin of the Korean Chemical Society Vol.32 No.9
Various aldoximes and ketoximes were efficiently reduced to their corresponding amines with NaBH_3CN in the presence of MoCl_5/NaHSO_4·H_2O system. Reduction reactions were carried out in refluxing EtOH or DMF within 0.3-3.8 h to afford the amines in high to excellent yields.
Behzad Zeynizadeh,Mehri Kouhkan 대한화학회 2011 Bulletin of the Korean Chemical Society Vol.32 No.9
Solvent-free reduction of various aldoximes and ketoximes to the corresponding amines was performed easily and efficiently with NaBH_4 in the presence of ZrCl_4 supported on Al_2O_3. The reactions were carried out rapidly (within 2 min) at room temperature to afford the amines in high to excellent yields.
Zeynizadeh, Behzad,Kouhkan, Mehri Korean Chemical Society 2011 Bulletin of the Korean Chemical Society Vol.32 No.9
Solvent-free reduction of various aldoximes and ketoximes to the corresponding amines was performed easily and efficiently with $NaBH_4$ in the presence of $ZrCl_4$ supported on $Al_2O_3$. The reactions were carried out rapidly (within 2 min) at room temperature to afford the amines in high to excellent yields.