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Fe-(Mo-Mn-P)-xSi계 합금의 성형밀도에 따른 소결거동
정우영,옥진욱,박동규,안인섭,Jung, Woo-Young,Ok, Jin-Uk,Park, Dong-Kyu,Ahn, In-Shup 한국분말야금학회 2017 한국분말재료학회지 (KPMI) Vol.24 No.5
The addition of a large amount of alloying elements reduces the compactibility and increases the compacting pressure, thereby shortening the life of the compacting die and increasing the process cost of commercial PM steel. In this study, the characteristic changes of Fe-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P alloys are investigated according to the Si contents to replace the expensive elements, such as Ni. All compacts with different Si contents are fabricated with the same green densities of 7.0 and $7.2g/cm^3$. The transverse rupture strength (TRS) and sintered density are measured using the specimens obtained through the sintering process. The sintered density tends to decrease, whereas the TRS increases as the Si content increases. The TRS of the sintered specimen compacted with $7.2g/cm^3$ is twice as high as that compacted with $7.0g/cm^3$.
P/M Fecralloy 성형체의 고온산화 및 전기저항 안정성에 미치는 SiO<sub>2</sub> 첨가 효과
박진우,옥진욱,정우영,박동규,안인섭,Park, Jin-Woo,Ok, Jin-Uk,Jung, Woo-young,Park, Dong-kyu,Ahn, In-Shup 한국분말야금학회 2017 한국분말재료학회지 (KPMI) Vol.24 No.4
A metallic oxide layer of a heat-resistant element contributes to the high-temperature oxidation resistance by delaying the oxidation and has a positive effect on the increase in electrical resistivity. In this study, green compacts of Fecralloy powder mixed with amorphous and crystalline silica are oxidized at $950^{\circ}C$ for up to 210 h in order to evaluate the effect of metal oxide on the oxidation and electrical resistivity. The weight change ratio increases as per a parabolic law, and the increase is larger than that observed for Fecralloy owing to the formation of Fe-Si, Fe-Cr composite oxide, and $Al_2O_3$ upon the addition of Si oxide. Si oxides promote the formation of $Al_2O_3$ and Cr oxide at the grain boundary, and obstruct neck formation and the growth of Fecralloy particles to ensure stable electrical resistivity.
Fe-(Mo,Mn)-P계 Lean alloy의 소결특성에 미치는 Si와 Sn의 영향
정우영,옥진욱,박동규,안인섭,Jung, Woo-Young,Ok, Jin-Uk,Park, Dong-Kyu,Ahn, In-Shup 한국분말야금학회 2018 한국분말재료학회지 (KPMI) Vol.25 No.4
A lean alloy is defined as a low alloy steel that minimizes the content of the alloying elements, while maintaining the characteristics of the sintered alloy. The purpose of this study is to determine the change in microstructure and mechanical properties due to the addition of silicon or tin in Fe-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P alloys. Silicon- or tin-added F-Mo-P, Fe-Mn-P, and Fe-Mo-Mn-P master alloys were compacted at 700 MPa and subsequently sintered under a $H_2-N_2$ atmosphere at $1120^{\circ}C$. The sintered density of three alloy systems decreases under the same compacting pressure due to dimensional expansion with increasing Si content. As the diffusion rate in the Fe-P-Mo system is higher than that in the Fe-P-Mn system, the decrease in the sintered density is the largest in the Fe-P-Mn system. The sintered density of Sn added alloys does not change with the increasing Sn content due to the effect of non-dimensional changes. However, the effect of Si addition on the transverse rupture strengthening enhancement is stronger than that of Sn addition in these lean alloys.