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Rod Milling과 Chemical Leaching에 의해 제작된 비평형 Al(Fe-Cu) 합금 분말의 결정화 및 자기적 특성
김현구,Kim Hyun-Goo 한국분말야금학회 2004 한국분말재료학회지 (KPMI) Vol.11 No.6
We report the crystallization and magnetic properties of non-equilibrium $Al_{0.6}(Fe_{x}Cu_{1-x})_{0.4}(x=0.25, 0.50, 0.75)$ alloy powders produced by rod-milling as well as by new chemical leaching. X-ray diffractometry, transmission electron microscopy, differential scanning calorimetry and vibrating sample magnetometry were used to characterize the as-milled and leached specimens. After 400 h or 500 h milling, only the broad peaks of nano bcc crystalline phases were detected in the XRD patterns. The crystallite size, the peak and the crystallization temperatures increased with increasing Fe. After being annealed at $600{^\circ}C$ for 1 h for as-milled alloy powders, the peaks of bcc $AlCu_{4}\;and\;Al_{13}Cu_{4}Fe_{3}\;for\;x=0.25,\;bcc\;AlCu_{4}\;and\;Al_{5}Fe_{2}\;for\;x=0.50,\;and\;Al_{5}Fe_{2},\;and\;Al_{0.5}Fe_{0.5}\;for\;x=0.75$ are observed. After being annealed at $500{^\circ}\;and\;600{^\circ}C$for 1 h for leached specimens, these non-equi-librium phases transformed into fcc Cu and $CuFe_{2}O_{4}$phases for the x=0.25 specimen, and into bcc ${\alpha}-Fe,\;fcc\;Cu,\;and\;CuFe_{2}O_{4}$ phases for both the x=0.50 and the x=0.75 specimens. The saturation magnetization decreased with increasing milling time for $Al_{0.6}(Fe_{x}Cu_{1-x})_{0.4}$ alloy powders. On cooling the leached specimens from $800{\~}850^{\circ}C$,\;the magnetization first sharply increase at about $491.4{\circ}C,\;745{\circ}C,\;and\;750.0{\circ}C$ for x=0.25, x=0.50, and x=0.75 specimens, repectively.
강동우,김현구 대한방사선 방어학회 1988 방사선방어학회지 Vol.13 No.2
CR-39 검출기를 부착한 두 종류의 라돈컵을 사용하여 토양중의 라돈 농도를 제주도 일원의 4개지역(제주시, 서귀포시, 대정읍, 성산읍)에서 측정하였다. 본 실험에서는 CR-39검출기의 최적 부식조건을 70f7, 6.25N NaOH, 5.5시간으로 결정하였으며, 두 종류의 라돈컵을 지금 15㎝, 깊이50㎝인 두개의 땅구덩이에 각각 설치하였는데 이중 밀폐된 라돈컵은 구덩이 바닥의 토양 위에, 개방된 라돈컵은 지지대를 이용하여 바닥에서 45㎝ 높이에 설치하였다. CR-39의 부식조건으로는 70℃의 6.25N NaOH 용액에서 5.5시간 동안 처리하였으며 환산인자로 1 track/㎟ㆍ30day=0.059Bq/ℓ을 얻었다. 1987년 5월 1일부터 1988년 4월 23일까지 측정한 결과 30일간의 평균 라돈 농도의 연평균치는 개방된 라돈컵과 밀폐된 라돈컵에서 각각 3.1±0.3Bq/ℓ와 1.7±0.2Bq/ℓ였다. A series of experiments is performed to measure radon concentration in the near-surface soil gas at the four locations (Cheju-Si, Seoguipo-Si, Taejeong-eup, Seongsan-eup) in Cheju Island, using CR-39 detectors placed inside radon cups. Two types of radon cups are installed in shallow holes of about 15㎝ in diameter and 50㎝ in depth. The optimum etching conditions, i.e., the concentration of NaOH solution, etchant temperature and etching time, are found to be 6.25N, 70℃ and 5.5 hours for CR-39 detectors. A typical conversion factor of radon cup is calculated as 1 track/㎟ㆍ30day=0.059Bq/ℓ. Average radon concentrations over 30 days measured in Cheju Island from May 1, 1987 to April 23, 1988 are 3.1±0.3Bq/ℓ for open radon cups and 1.7±0.2Bq/ℓ for closed radon cups.
Rod Milling에 의해 제작된 비평형 Al(Fe-Cu) 합금 분말의 형성 및 Chemical Leaching
김현구,명화남 한국분말야금학회 2002 한국분말재료학회지 (KPMI) Vol.9 No.5
We report the structure, thermal and magnetic properties of a non-equilibrium $Al_{0.6}(Fe_{50}Cu_{50})_{0.4}$ alloy powder produced by rod milling and chemical leaching. An X-ray diffractometry(XRD), a transmission electron microscope(TEM), a differential scanning calorimeter(DSC), a vibrating sample magnetometer(VSM), and superconducting quantum interference device(SQUID) were utilized to characterize the as-milled and leaching specimens. The crystallite size reached a value of about 8.82 nm. In the DSC experiment, the peak temperatures and crystallization temperatures decreased with increasing milling time. The activation energy of crystallization is 200.5 kJ/mole for as-milled alloy powder. The intensities of the XRD peaks of as-milled powders associated with the bcc type $Al_{0.5}Fe_{0.5}$ structure formative at $350^{\circ}C$ sharply increase with increasing annealing temperature. Above $400^{\circ}C$, peaks alloted to $Al_{0.5}Fe_{0.5}$ and $Al_{5}Fe_{2}$ are observed. After annealing at $600^{\circ}C$ for 1h, the leached Ll specimen transformed into bcc $\alpha$-Fe and fcc Cu phases, accompanied by a change in the structural and magnetic properties. The saturation magnetization decreased with increasing milling time, and a value of about 8.42 emu/g was reached at 500 h of milling. The coercivity reached a maximum value of about 142.7 Oe after 500 h of milling. The magnetization of leached specimens as function of fields were higher at 5 K, and increased more sharply at 5 K than at 100 K.
연결 강판을 이용한 모듈러 유닛 간 접합부의 비선형 거동 해석
김현구,유정한 한국공간구조학회 2023 한국공간구조학회지 Vol.23 No.2
Modular construction is an economical and efficient construction that reduces time and costs by manufacturing units in factories and constructing them on site. Currently, the demand for modular construction is increasing not only abroad but also domestically. As the demand for modular construction increases, a lot of development and research on connections between modular units are being conducted. Connections between modular units should be quick and simple to assemble when assembling units on site, and should be in a form that allows each unit to be connected regardless of direction. In addition, it must be able to exert sufficient strength against external loads. In this study, a connection between modular units using connecting steel plates and bolts was proposed, and the nonlinear behavior of the connection to external lateral force was analyzed through finite element analysis, and resistance performance was evaluated.