Taxol 합성에 관한 연구 Ⅰ : O-(tert-Butyldiphenylsily1)-cis-5-methyl-4-hepten-6-yn-1-ol의 합성 Synthesis of O-(tert-Butyldiphenylsily1)-cis-5-methyl-4-hepten-6-yn-1-ol

신동수,박두천,주우홍,김형국 國立 昌原大學校 基礎科學硏究所 1994 基礎科學硏究所論文集 Vol.6 No.-

O-(tert-Butyldiphenylsily1)-cis-5-methyl-4-hepten-6-yn-1-ol, an intermediate in the synthesis of taxol, was efficiently synthesized from 3-methyl-2-penten-4-yn-1-ol by sequential alcohol/bromide interchange [NBS, PPh_(3), CH_(2)Cl_(2), -30℃, 82%], displacement with the lithium salt of tert-butylacetate [LDA, THF, -78 to 23℃, 84%], LAH reduction, and silylation [tBuPhSiCl, imidazole, CH_(2)Cl_(2), 45℃, 88%].

단섬유강화 무기 복합재료의 파괴인성에 관한 연구

신익재,이동주 영남대학교 공업기술연구소 1999 工業技術硏究所論文集 Vol.27 No.1

The objective of paper is to study the reinforcing effects of fiber volume fraction and aspect ratio in short-fiber filled ceramic matrix composites. The parameters of fracture mechanics, K and J are applied to assess fracture toughness and bridging effect. It is found that fracture toughness is greatly influenced by the fiber bridging, Also, the nonlinear fracture analysis such as J-integral is more effective than LEFM for short-fiber reinforced ceramic matrix composites. For the reinforcing effects as functions of fiber volume fraction and aspect ratio, fracture toughness is increased rapidly with fiber volume fraction and aspect ratio as expected.

再建築의 問題點과 改善方案에 關한 硏究

申東柱 건국대학교 1995 政治論叢 Vol.30 No.-

광섬유 집합체 센서를 이용한 6MV 광자선의 반음영 및 심부선량백분율 측정

신상훈,장경원,조동현,유욱재,서정기,이봉수,문주현,박병기 제주대학교 방사선응용과학연구소 2008 방사선응용과학연구소논문집 Vol.22 No.-

In this study, a fiber-optic bundle sensor has been developed using water-equivalent organic scintillating fibers for photon beam measurement. Beam penumbra and percent depth doses(PDD) are measured according to the depth of the photon beam. This sensor has many advantages such as high resolution, real-time measurement and ease of calibration over conventional radiation measurement devices.

재발성 류마티즘 환자에서 발작의 유발인자

주유철,이동민,양종태,신병철,임태영,서정균,정기영,최동헌,김원,조영신,고희관 조선대학교 2001 The Medical Journal of Chosun University Vol.26 No.2

Background and Objectives : Palindromic rheumatism (PR) is known to be triggered without any obviously inciting events in most patients, although, in a few cases, attacks have been noted to relate to another events such as weather change, childbirth, ingestion of certain foods, or over-exercise. The aim of this study was to characterize the triggering factors on palindromic attacks. Materials and Methods : We evaluated sixty-four patients with PR for the presence of triggering factors and the relationship between attacks and triggering factors by interview of patients. We considered that there was an probable association between episodes and PR, if episodes within 24 hours prior to PR had triggered at least 50% of all attacks and a definite association between episodes and PR, if episodes within 24 hours prior to PR had triggered 100% of all attacks. Results : In 15 patients (35.9%), there was a possible association between episodes of PR and initiating events. In 8 patients (12.5%), there was a definite association between episodes of PR and initiating events. The triggering factors were physical over-activity including exercise (19/64: 29.7%), foods, such as rawfish, crab, and chicken, including alcohol (19/96: 19.8%). However, there were no difference between the groups with and without the triggering factor in sex ratio, duration and onset of PR, the positive rate of rheumatoid factor and involved sites. Conclusion : Our observations showed that PR was triggered by physical over-activity more than in previous reports and hypersensitivity to foods was a causative factor in some patients with PR. However, patients with triggering factors had a similiar clinical profile to patients without triggering factors.

희생양극을 이용한 자동차 소음기의 음극방식에 관한 연구

신동호,심재주,최윤석,김정구 대한금속재료학회 2004 대한금속·재료학회지 Vol.42 No.12

In order to apply a sacrificial anode cathodic protection system for automotive muffler materials, determination of reliable sacrificial anode and its protection ability were evaluated by laboratory tests in synthetic condensed water. Three kinds of sacrificial anodes were selected: aluminum (AI), zinc (Zn) and magnesium (Mg), and the muffler materials were Al-coated steel and uncoated steel. The corrosion behavior in synthetic condensed water for the muffler materials and sacrificial anodes was investigated by potentiodynamic tests. The cathodic protection ability was evaluated by galvanic corrosion test and weight-loss test. The results of the potentiodynamic test indicated that Al was less suitable for sacrificial anode because it became passive. Mg was also unqualified due to the high dissolution rate. However, Zn was adequate for sacrificial anode because of its low dissolution rate, high stability and suitable potential difference. Results of weight-loss test demonstrated that the corrosion rate of Al-coated steel was reduced from 0.028 to 0.018 mm/year, and that of uncoated steel was 0.08 to 0.002 mm/year by coupling with Zn anode. In addition, the proper area ratio of anode to cathode was 1 : 10. From these results, it can be concluded that Zn anode can protect both the Al-coating with passivation, and steel substrate with low dissolution rate. (Received January 8, 2004)

감마선투과검사 장치의 자동 원격조작기 개발

주광태,신진성,김동언,송정호,주승환,장홍근 한국비파괴검사학회 2002 한국비파괴검사학회지 Vol.22 No.5

국내 감마선투과검사용 조사장치는 1,000여대로 2,500여명의 종사자가 대부분 수동으로 원격 조작하는 실정으로 작업의 효율화와 방사선피폭 저감화를 위하여 자동 원격조작기의 사용이 요구된다. 이에 연구팀은 실무에 적합한 토크와 안전계수로부터 54kgf·㎝의 출력을 지닌 24V, 200W의 BLDC모터를 이용하여 0.4∼1.2 m/s 범위의 선원 이동속도를 조절할 수 있는 구동장치와 RF 센서로 구동 속도 조절, 광전센서에 의한 선원 위치 및 timer로 노출시간을 제어할 수 있는 무선 원격조작기를 개발하였다. 이와 같이 개발한 자동원격조작기는 AC와 DC 겸용, 그리고 기존의 수동 원격조작기에 탈착이 가능하여 자동과 수동을 겸용할 수 있는 경제적 이점 등으로 활용도가 클 것으로 기대된다. Recently, gamma radiographic equipments have been used about 1,000 sets manually and operated by about 2,500 persons in Korea. In order for a radiography to work effectively with avoiding any hazard of the high level radiation from the source, many field workers have expected developing a wireless automatic remote exposure controller. The KITCO research team has developed an automatic remote exposure controller that can regulate the speed of 0.4∼1.2 m/s by BLDC motor of 24V 200W which has output of 54 kgf·㎝, suitable torque and safety factor for the work. And the developed automatic remote exposure controller can control rpm of motor, pigtail position by photo-sensor and exposure time by timer to RF sensor. Thus, the developed equipment is expected that the unit can be used in many practical applications with benefits in economical advantage to combine the use of both automatic and manual type because attachment is possible existent manual remote exposure controller, AC and DC combined use.

대학생의 전공 계열별 스포츠 가치의식에 미치는 변인에 관한 연구

신영균,주동욱 한국스포츠리서치 2004 한국 스포츠 리서치 Vol.15 No.1

The purpose of this study is to investigate the effects on the Value Consciousness in Sports of University Students by Special study. This study is to analyze and clarify the effects of the sport experience, A school year, soundness, to be weighty of sport. For the study 323 sports and 333non-sports participation were selected (totaled 656 university students 342, college students 314). statistical analysis techniques for this study included factor analysis, reliability analysis, one-way ANOVA, correlation analysis, multiple regression analysis, x². Based on findings of these analysis the results of the study are as follow: First, there were differences on the Value Consciousness in Sports of University Students by Special study. The arts and sports Special study is higher to become visible. Second, The effects on the Value Consciousness in Sports is Social intercourse of Civilization, a body. of Natural science, Social intercourse of arts and sports Special study. Third, The frequency in use of a sport Participation is Arts and sports Special study 5 a week(29.7%). Fourth, Consciousness in Health is Civilization 53.3%, Natural science 47.6%, arts and sports Special study65.99% with to become visible. Fifth, Consciousness to be weighty of sport is Arts and sports Special study 5 a week(29.7%). Fourth, Consciousness in Health is Civilization 49.2%, Natural science 40.0%, arts and sports Special study 59.4% with to become visible.

장기간 보관한 멸균물품의 오염 상태에 관한 연구

주홍순,조순덕,정재심,신동분,임바올라,노은지,이선희,송영미,최정화,백병윤,김미나 대한병원감염관리학회 2003 의료관련감염관리 Vol.8 No.1

글로우 방전을 이용한 이산화탄소의 전환특성

신용섭,송승훈,곽동주 慶星大學校 1998 論文集 Vol.19 No.2

In this study, the characteristics of CO₂conversion and glow discharge were investigated using glow discharge plasma reactor with a parallel copper electrode system. A pure CO₂ gas was used for the carrier gas under gas pressure of 10∼80 torr in a glow discharge. For glow discharge, discharge current was increased with the increase of discharge voltage. In the case of constant discharge voltage, the discharge current tend to increase with the decreasing of gas pressure. Using pure CO₂only, the CO₂conversion was increased with the increase of discharge power and the decreased of gas pressure. The maximum CO₂ conversion was 28% at 10 torr, 598 W, 902.4V. Energy yield was decreased with the increase of discharge power and discharge voltage. Also, the concentrations of CO₂and O₂in the produced gas were slightly increased with the increase of CO₂ conversion.