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      대기 중 다환방향족탄화수소 측정방법의 성능평가 - 하이볼륨 샘플링 및 GC/MS 분석방법을 대상으로 = Evaluation of a Method for the Measurement of PAHs in the Ambient Atmosphere - Focusing on High Volume Sampling and GC/MS Analysis

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      https://www.riss.kr/link?id=A103755050

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      다국어 초록 (Multilingual Abstract)

      In this study, a measurement method was evaluated for the determination of polycyclic aromatic hydrocarbons (PAHs) in the ambient atmosphere. PAHs were sampled by high-volume samplers, and were then analysed with a GC/MS system. Particulate PAHs were ...

      In this study, a measurement method was evaluated for the determination of polycyclic aromatic hydrocarbons (PAHs) in the ambient atmosphere. PAHs were sampled by high-volume samplers, and were then analysed with a GC/MS system. Particulate PAHs were collected on $8"{\times}10"$ quartz fiber filter, while vapor phase PAHs were adsorbed on polyurethane foam (PUF). Target compounds included a total of 36 PAHs, which are known to be frequently detected in the urban atmosphere. It was not necessary to clean-up samples before samples were analyzed using GC/MS, and the overall performance of the method was tested by a variety of quality control and quality assurance schemes. It is generally known that the clean-up procedure can negatively affect the recovery of samples. Precision and accuracy was evaluated using SRM provided by US NIST, and the results were generally satisfactory and reliable. However, the GC/MS method appeared not to be adequate for 6-rings PAHs, such as coronene, due to its lower sensitivity. In addition, collection efficiencies for low molecular compounds, such as 2-rings PAHs, were poor because of the lower retention volume of the PUF adsorbent. As a result, it was concluded that the method based on high-volume sampling and GC/MS analysis can give very reliable data by simultaneous sampling of both particulate and vapor phases for 3-rings to 5-rings PAHs of environmental concern.

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      참고문헌 (Reference)

      1 백성옥, "대기환경측정과 정도관리(Ⅰ) - 원리와 방법론" 한국대기환경학회 20 (20): 237-249, 2004

      2 이민도, "대기 중 다환방향족탄화수소(PAHs)의 측정?분석신뢰도 향상에 관한 고찰" 한국대기환경학회 23 (23): 515-525, 2007

      3 Kim, S. C., "Trends in concentration of polycyclic aromatic hydrocarbons of PM-10 in Suwon area" 12 (12): 341-350, 1996

      4 Glaser, J. A., "Trace analysis for wastewaters" 15 (15): 1426-1435, 1981

      5 ATSDR, "Toxicological profile for polycyclic aromatic hydrocarbons" 2-6, 1995

      6 Maddalena, R. L., "Simple and rapid extraction of polycyclic aromatic hydrocarbons collected on polyurethane foam adsorbent" 32 (32): 2497-1503, 1998

      7 Chung, Y., "Seasonal variation of size distributions of polycyclic aromatic hydrocarbons in air particulates" 14 (14): 577-588, 1998

      8 Baek, S. O., "Occurrence and behaviour of polycyclic aromatic hydrocarbons in the ambient air(I) - Locational and seasonal concentrations" 18 (18): 465-480, 1996

      9 ASC committee, "Guidelines for data acquisition and data quality evaluation in environmental chemistry" 52 (52): 2242-2249, 1980

      10 Phillips, D. H., "Fifty years of benzo(a)pyrene" 303 (303): 468-472, 1983

      1 백성옥, "대기환경측정과 정도관리(Ⅰ) - 원리와 방법론" 한국대기환경학회 20 (20): 237-249, 2004

      2 이민도, "대기 중 다환방향족탄화수소(PAHs)의 측정?분석신뢰도 향상에 관한 고찰" 한국대기환경학회 23 (23): 515-525, 2007

      3 Kim, S. C., "Trends in concentration of polycyclic aromatic hydrocarbons of PM-10 in Suwon area" 12 (12): 341-350, 1996

      4 Glaser, J. A., "Trace analysis for wastewaters" 15 (15): 1426-1435, 1981

      5 ATSDR, "Toxicological profile for polycyclic aromatic hydrocarbons" 2-6, 1995

      6 Maddalena, R. L., "Simple and rapid extraction of polycyclic aromatic hydrocarbons collected on polyurethane foam adsorbent" 32 (32): 2497-1503, 1998

      7 Chung, Y., "Seasonal variation of size distributions of polycyclic aromatic hydrocarbons in air particulates" 14 (14): 577-588, 1998

      8 Baek, S. O., "Occurrence and behaviour of polycyclic aromatic hydrocarbons in the ambient air(I) - Locational and seasonal concentrations" 18 (18): 465-480, 1996

      9 ASC committee, "Guidelines for data acquisition and data quality evaluation in environmental chemistry" 52 (52): 2242-2249, 1980

      10 Phillips, D. H., "Fifty years of benzo(a)pyrene" 303 (303): 468-472, 1983

      11 Baek, S. O., "Effect o f ambient temperature on the distribution of atmospheric concentrations of polycyclic aromatic hydrocarbons in the vapor and particulate phases" 14 (14): 117-131, 1998

      12 Baek, S. O., "E valuation o f sampling methodology for the Measurement of Polycyclic aromatic hydrocarbons in the atmosphere" 14 (14): 43-62, 1998

      13 Seo, Y. H., "Determination of polycyclic aromatic hydrocarbons in chimney soot extract by high-resolution gas chromatography" 4 (4): 11-19, 1988

      14 Baek, S. O., "Determination of polycyclic aromatic hydrocarbons associated with airborne particulate matter using HPLC and Fluorescence Detection" 17 (17): 85-99, 1995

      15 USEPA, "Definition and procedure for the determination of the method detection limit, 40 CFR Part 136(analytical procedure), appendix B, 319"

      16 USEPA, "Compendium Method TO-17, Determination of volatile organic compounds in ambient air using active sampling onto sorbent tubes, 2nd. Ed" 1999

      17 USEPA, "Compendium Method TO-13A, Determination of polycyclic aromatic hydrocarbons in ambient air using gas chromatography/mass spectrometry, 2nd. Ed" 1999

      18 Ravindra, K., "Atmospheric polycyclic hydrocarbons: Source attribution, emission factors and regulation" 42 (42): 2895-2921, 2008

      19 Baek, S. O., "Atmospheric polycyclic aromatic hydrocarbons - Environmental implications" 15 (15): 525-544, 1999

      20 IARC, "Agents reviewed by the IARC monographs. volumes 1-99"

      21 Pyo, H. S., "A study on the analysis of polycyclic aromatic hydrocarbons in air" 13 (13): 453-465, 2000

      22 Park, C. K., "A comparative study on the analytical methods of polycyclic aromatic hydrocarbons in the atmosphere" 16 (16): 595-606, 2000

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      학술지 이력

      학술지 이력
      연월일 이력구분 이력상세 등재구분
      2022 평가예정 계속평가 신청대상 (등재유지)
      2017-01-01 평가 우수등재학술지 선정 (계속평가)
      2013-01-01 평가 등재 1차 FAIL (등재유지) KCI등재
      2010-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2008-02-15 학술지명변경 외국어명 : Korean Journal of Environmental Health -> JOURNAL OF ENVIRONMENTAL HEALTH SCIENCES KCI등재
      2008-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2006-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2005-09-13 학술지등록 한글명 : 한국환경보건학회지
      외국어명 : Korean Journal Of Environmental Health
      KCI등재
      2005-06-02 학술지등록 한글명 : 한국환경보건학회지
      외국어명 : Korean Journal of Environmental Health
      KCI등재
      2005-01-27 학회명변경 한글명 : 한국환경위생학회 -> 한국환경보건학회
      영문명 : Korean Society Of Environmental Health -> Korean Society of Environmental Health
      KCI등재
      2003-01-01 평가 등재학술지 선정 (등재후보2차) KCI등재
      2002-01-01 평가 등재후보 1차 PASS (등재후보1차) KCI등재후보
      1999-01-01 평가 등재후보학술지 선정 (신규평가) KCI등재후보
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      학술지 인용정보

      학술지 인용정보
      기준연도 WOS-KCI 통합IF(2년) KCIF(2년) KCIF(3년)
      2016 0.44 0.44 0.4
      KCIF(4년) KCIF(5년) 중심성지수(3년) 즉시성지수
      0.42 0.4 0.605 0.21
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