검정콩 종피에 함유된 안토시아닌의 색소별 함량을 비파괴적으로 신속하게 분석하기 위하여 NIRS(근적외선 분광분석기)를 이용한 모델을 개발하였다. 재료는 검정콩 유전자원 300 계통을 사...
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https://www.riss.kr/link?id=A100200559
2008
Korean
NIRS ; anthocyanin ; soybean ; HPLC ; MPLS regression
524.2
KCI등재
학술저널
15-20(6쪽)
4
0
상세조회0
다운로드국문 초록 (Abstract)
검정콩 종피에 함유된 안토시아닌의 색소별 함량을 비파괴적으로 신속하게 분석하기 위하여 NIRS(근적외선 분광분석기)를 이용한 모델을 개발하였다. 재료는 검정콩 유전자원 300 계통을 사...
검정콩 종피에 함유된 안토시아닌의 색소별 함량을 비파괴적으로 신속하게 분석하기 위하여 NIRS(근적외선 분광분석기)를 이용한 모델을 개발하였다. 재료는 검정콩 유전자원 300 계통을 사용하였으며, HPLC에서 분석된 종피의 안토시아닌 함량치를 NIRS 스펙트럼에 적용시킨 후 검량식을 작성하였다. NIRS의 검량식을 몇 가지 방법에 의하여 비교 분석한 결과 1차미분된 스펙트럼을 MPLS(Modified Partial Least Squares)를 이용한 회귀식에 이용하는 것이 가장 적합하였다. HPLC를 이용한 유전자원들의 성분 함량과 NIRS에서 도출된 검량식과의 상관계수는 C3G, D3G 및 Pt3G가 각각 0.952, 0.936과 0.833을 나타내었다. 이들 검량식은 validation file에서도 C3G와 D3G는 0.897, 0.849의 높은 상관을 보였으며, 이는 NIRS를 이용하여 검정콩의 안토시아닌 함량을 신속하게 분석할 수 있음을 나타내는 것으로 판단되었다.
다국어 초록 (Multilingual Abstract)
Near infrared reflectance spectroscopy (NIRS) is a rapid and accurate analytical method for determining the composition of agricultural products and feeds. This study was conducted to measure anthocyanin contents in black colored soybean by using NIRS...
Near infrared reflectance spectroscopy (NIRS) is a rapid and accurate analytical method for determining the composition of agricultural products and feeds. This study was conducted to measure anthocyanin contents in black colored soybean by using NIRS system. Total 300 seed coat of black colored soybean samples previously analyzed by HPLC were scanned by NIRS and over 250 samples were selected for calibration and validation equation. A calibration equation calculated by MPLS(modified partial least squares) regression technique was developed in which the coefficient of determination for anthocyanin pigment C3G, D3G and Pt3G content was 0.952, 0.936, and 0.833, respectively. Each calibration equation was applied to validation set that was performed with the remaining samples not included in the calibration set, which showed high positive correlation both in C3G and D3G content file. In case Pt3G, the prediction model was needed more accuracy because of low R2 value in validation set. This results demonstrate that the developed NIRS equation can be practically used as a rapid screening method for quantification of C3G and D3G contents in black colored soybean.
참고문헌 (Reference)
1 권영립, "벼 생체엽신 질소함량 측정을 위한 근적외선분광분석의 검량식 작성" 한국작물학회 50 (50): 394-399, 2005
2 Kwan Su Kim, "Use of Near-Infrared Spectroscopy for Estimating Fatty Acid Composition in Intact Seeds of Rapeseed" 한국작물학회 10 (10): 15-20, 2007
3 Velasco, L., "Screening ethiopian mustard for erucic acid by near infrared reflectance spectroscopy" 36 : 1068-1071, 1996
4 Fuleki, T, "Quantitative methods for anthocyanins. l. Extraction and determination of total antocyanin in cranberries" 33 : 254-259, 1968
5 김용호, "NIRS를 이용한 삼지구엽초의 이카린 함량 분석" 한국약용작물학회 10 (10): 340-343, 2002
6 Choung, M. G., "Isolation and determination of anthocyanins in seed coats of black soybean" 49 : 5848-5851, 2001
7 Martin, W, "High-pressure liquid chromatographic seperation of 3-glucoside, 3,5-diglucosides, 3- (6-O-p-coumaryl)glucosides and 3-(6-O-p-coumarylglucoside)- 5-glucosides of anthocyanidins" 155 : 389-398, 1978
8 Francis,F.J, "Food Colorants: Anthocyanins" 28 : 273-314, 1989
9 Havsteen,B, "Flavonoids: a class of natural products of high pharmacological potency" 32 : 1141-1145, 1983
10 Kim, S. L., "Extraction, purification and quantification of anthocyanins in colored rice, black soybean, and black waxy corn" 32 (32): 146-152, 2000
1 권영립, "벼 생체엽신 질소함량 측정을 위한 근적외선분광분석의 검량식 작성" 한국작물학회 50 (50): 394-399, 2005
2 Kwan Su Kim, "Use of Near-Infrared Spectroscopy for Estimating Fatty Acid Composition in Intact Seeds of Rapeseed" 한국작물학회 10 (10): 15-20, 2007
3 Velasco, L., "Screening ethiopian mustard for erucic acid by near infrared reflectance spectroscopy" 36 : 1068-1071, 1996
4 Fuleki, T, "Quantitative methods for anthocyanins. l. Extraction and determination of total antocyanin in cranberries" 33 : 254-259, 1968
5 김용호, "NIRS를 이용한 삼지구엽초의 이카린 함량 분석" 한국약용작물학회 10 (10): 340-343, 2002
6 Choung, M. G., "Isolation and determination of anthocyanins in seed coats of black soybean" 49 : 5848-5851, 2001
7 Martin, W, "High-pressure liquid chromatographic seperation of 3-glucoside, 3,5-diglucosides, 3- (6-O-p-coumaryl)glucosides and 3-(6-O-p-coumarylglucoside)- 5-glucosides of anthocyanidins" 155 : 389-398, 1978
8 Francis,F.J, "Food Colorants: Anthocyanins" 28 : 273-314, 1989
9 Havsteen,B, "Flavonoids: a class of natural products of high pharmacological potency" 32 : 1141-1145, 1983
10 Kim, S. L., "Extraction, purification and quantification of anthocyanins in colored rice, black soybean, and black waxy corn" 32 (32): 146-152, 2000
11 Kim, Y. H., "Extraction and separation of anthocyanins in black soybean" 39 : 35-38, 1997
12 Choi, H. C, "Develolment and industrial utilization of natural pigments from colored rices" NCES, RDA 1996
13 Lee, H. B., "Determination of seed protein and oil concentration in kiddny bean by near infrared spectroscopic analysis" 46 (46): 248-252, 2001
14 Daun, J. K., "Comparison of three whole seed near-infrared analyzers for measuring quality components of canola seed" 71 (71): 1063-1068, 1994
15 Kim, Y. H., "Antioxidant activity and extraction efficiency of anthocyanin pigments in black colored soybean" 23 (23): 1-9, 2006
16 Yoshikura, K, "Anthocyanins of the black soybean" 22 : 367-, 1969
17 Jung, C. S., "Analysis of protein and moisture contents in pea using near-infrared reflectance spectroscopy" 43 (43): 101-104, 1998
18 Williams, P. C., "Analysis of oat bran products by near infrared reflectance spectroscopy" 36 (36): 571-574, 1991
19 Bae E. A, "A study of the antioxidative activities of Korean soybeans" 26 : 203-208, 1997
Evaluation of Agronomic Stability of North Korean Rice Varieties using Statistical Models
Simulating Ammonia Volatilization from Applications of Different Urea Applied in Rice Field by WNMM
Effects of Elevated CO₂ on Maize Growth
원료콩의 저장 기간과 방법이 콩나물의 생장에 미치는 영향
학술지 이력
연월일 | 이력구분 | 이력상세 | 등재구분 |
---|---|---|---|
2028 | 평가예정 | 재인증평가 신청대상 (재인증) | |
2022-01-01 | 평가 | 등재학술지 유지 (재인증) | |
2019-01-01 | 평가 | 등재학술지 유지 (계속평가) | |
2016-01-01 | 평가 | 등재학술지 선정 (계속평가) | |
2015-12-01 | 평가 | 등재후보로 하락 (기타) | |
2011-01-01 | 평가 | 등재 1차 FAIL (등재유지) | |
2009-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2007-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2005-01-01 | 평가 | 등재학술지 유지 (등재유지) | |
2002-01-01 | 평가 | 등재학술지 선정 (등재후보2차) | |
1999-07-01 | 평가 | 등재후보학술지 선정 (신규평가) |
학술지 인용정보
기준연도 | WOS-KCI 통합IF(2년) | KCIF(2년) | KCIF(3년) |
---|---|---|---|
2016 | 0.46 | 0.46 | 0.42 |
KCIF(4년) | KCIF(5년) | 중심성지수(3년) | 즉시성지수 |
0.49 | 0.49 | 0.91 | 0.08 |