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      Hierarchically Porous Aminosilica Monolith as a CO<sub>2</sub> Adsorbent

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      https://www.riss.kr/link?id=A107644193

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      <P>A facile strategy is successfully developed for the centimeter-scale preparation of hierarchically porous aminosilica monolith as a CO<SUB>2</SUB> adsorbent just by simple processes of solvent-evaporation-induced coating, self-assembly, and concentration of tetraethyl orthosilicate sol on the surface of a polymer foam template without any adhesive composite material or hydrothermal treatment. (3-Aminopropyl) trimethoxysilane is immobilized on the surface of silica monolith via a gas-phase procedure. The silica frameworks of the monolith mimic those of the polymer foam template at the macroscale, and the frameworks are composed of the SBA-15 structure at the nanoscale. The hierarchically porous structure demonstrates improved properties over the single-mode porous component, with the macroporous framework ensuring mechanical stability and good mass transport properties, while the smaller pores provide the functionality for CO<SUB>2</SUB> adsorption.</P><P><B>Graphic Abstract</B>
      <IMG SRC='http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/aamick/2014/aamick.2014.6.issue-15/am5029022/production/images/medium/am-2014-029022_0010.gif'></P>
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      <P>A facile strategy is successfully developed for the centimeter-scale preparation of hierarchically porous aminosilica monolith as a CO<SUB>2</SUB> adsorbent just by simple processes of solvent-evaporation-induced coating, self-ass...

      <P>A facile strategy is successfully developed for the centimeter-scale preparation of hierarchically porous aminosilica monolith as a CO<SUB>2</SUB> adsorbent just by simple processes of solvent-evaporation-induced coating, self-assembly, and concentration of tetraethyl orthosilicate sol on the surface of a polymer foam template without any adhesive composite material or hydrothermal treatment. (3-Aminopropyl) trimethoxysilane is immobilized on the surface of silica monolith via a gas-phase procedure. The silica frameworks of the monolith mimic those of the polymer foam template at the macroscale, and the frameworks are composed of the SBA-15 structure at the nanoscale. The hierarchically porous structure demonstrates improved properties over the single-mode porous component, with the macroporous framework ensuring mechanical stability and good mass transport properties, while the smaller pores provide the functionality for CO<SUB>2</SUB> adsorption.</P><P><B>Graphic Abstract</B>
      <IMG SRC='http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/aamick/2014/aamick.2014.6.issue-15/am5029022/production/images/medium/am-2014-029022_0010.gif'></P>

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