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        Key Characteristics of a Novel Silk Yarn from Fresh Cocoons

        Qifan Xie,Haiping Zhang,Mingying Yang,Liang-Jun Zhu 한국섬유공학회 2018 Fibers and polymers Vol.19 No.1

        We studied the key characteristics of a novel silk yarn reeled from fresh cocoons. Compared with traditional silk yarn, this novel silk yarn displayed better mechanical properties, especially in terms of a higher breaking stress and toughness, and exhibited a different surface morphology. A cross-sectional observation and the sericin content results illustrated that different sericin coatings on the silk yarn reeled from fresh cocoons surface did not improve the mechanical properties. The degumming and tensile testing analysis indicated that degummed silk fibroin of novel silk yarn is able to resist deformation and fracture better than silk fibroin of traditional silk yarn. The FTIR results revealed that the selected techniques is an important contributor to the silk fibroin mechanical properties, because novel technique brought higher percentage beta-sheet structures in novel silk yarn fibroin than traditional silk yarn. The new technique that using novel silkyarn has improved its mechanical properties and it is expected that the silk yarn with superior mechanical properties could be used in fabrics transistors, electrodes and reinforced biomaterials.

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        High solid content 45S5 bioglass®-based scaffolds using stereolithographic ceramic manufacturing: process, structural and mechanical properties

        Zhiyong Ma,Jun Xie,Xian Zhen Shan,Jiabin Zhang,Qifan Wang 대한기계학회 2021 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.35 No.2

        45S5 Bioglass® has been widely used in bone tissue engineering scaffold due to its high bioactive properties. 3D printing method is a popular way to fabricate scaffolds. The extrusion printing method causes poor shape and dimensional accuracy of the scaffolds. The ordinary light-cured 3D printing method leads to low solid content of the scaffolds, which causes large shape shrinkages and low mechanical properties after sintering. In this study, we employed the stereolithographic ceramic manufacturing (SLCM) method to fabricate 45S5 Bioglass®-based scaffolds. Coating-then-stereolithographic layer by layer is the core process of SLCM method. Based on the optimization of the parameters of SLCM process and sintering process, the solid content of the 45S5 scaffold can be improved to a maximum of 70 %, and the linear shrinkage and compressive strength were effectively improved. The proposed method can be used not only for fabricating bone tissue engineering scaffold, but also for manufacturing other high solid content ceramic products.

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