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김현구,Kim, Hyun-Goo 한국분말야금학회 2009 한국분말재료학회지 (KPMI) Vol.16 No.5
The amorphization process and the thermal properties of amorphous Ti$_{40}$Cu$_{40}$Ni$_{10}$Al$_{10}$ powder during milling by mechanical alloying were examined by X-ray diffractometry (XRD), differential scanning calorimetry (DSC), and transmission electron microscopy (TEM). The chemical composition of the samples was examined by an energy dispersive X-ray spectrometry (EDX) facility attached to the scanning electron microscope (SEM). The as-milled powders showed a broad peak (2$\theta$ = 42.4$^{\circ}$) with crystalline size of about 5.0 nm in the XRD patterns. The entire milling process could be divided into three different stages: agglomeration (0 < t$_m$ $\leq$ 3 h), disintegration (3 h < t$_m$ $\leq$ 20 h), and homogenization (20 h < t$_m$ $\leq$ 40 h) (t$_m$: milling time). In the DSC experiment, the peak temperature T$_p$ and crystallization temperature T$_x$ were 466.9$^{\circ}C$ and 444.3$^{\circ}C$, respectively, and the values of T$_p$, and T$_x$ increased with a heating rate (HR). The activation energies of crystallization for the as-milled powder was 291.5 kJ/mol for T$_p$.
Rod Milling과 Chemical Leaching에 의해 제작된 비평형 Al(Fe-Cu) 합금 분말의 결정화 및 자기적 특성
김현구,Kim Hyun-Goo 한국분말야금학회 2004 한국분말재료학회지 (KPMI) Vol.11 No.6
We report the crystallization and magnetic properties of non-equilibrium $Al_{0.6}(Fe_{x}Cu_{1-x})_{0.4}(x=0.25, 0.50, 0.75)$ alloy powders produced by rod-milling as well as by new chemical leaching. X-ray diffractometry, transmission electron microscopy, differential scanning calorimetry and vibrating sample magnetometry were used to characterize the as-milled and leached specimens. After 400 h or 500 h milling, only the broad peaks of nano bcc crystalline phases were detected in the XRD patterns. The crystallite size, the peak and the crystallization temperatures increased with increasing Fe. After being annealed at $600{^\circ}C$ for 1 h for as-milled alloy powders, the peaks of bcc $AlCu_{4}\;and\;Al_{13}Cu_{4}Fe_{3}\;for\;x=0.25,\;bcc\;AlCu_{4}\;and\;Al_{5}Fe_{2}\;for\;x=0.50,\;and\;Al_{5}Fe_{2},\;and\;Al_{0.5}Fe_{0.5}\;for\;x=0.75$ are observed. After being annealed at $500{^\circ}\;and\;600{^\circ}C$for 1 h for leached specimens, these non-equi-librium phases transformed into fcc Cu and $CuFe_{2}O_{4}$phases for the x=0.25 specimen, and into bcc ${\alpha}-Fe,\;fcc\;Cu,\;and\;CuFe_{2}O_{4}$ phases for both the x=0.50 and the x=0.75 specimens. The saturation magnetization decreased with increasing milling time for $Al_{0.6}(Fe_{x}Cu_{1-x})_{0.4}$ alloy powders. On cooling the leached specimens from $800{\~}850^{\circ}C$,\;the magnetization first sharply increase at about $491.4{\circ}C,\;745{\circ}C,\;and\;750.0{\circ}C$ for x=0.25, x=0.50, and x=0.75 specimens, repectively.
김현구(Kim, Hyun-Goo),우상우(Woo, Sang-Woo),장문석(Jang, Moon-Seok),신형기(Shin, Hyung-Ki) 한국신재생에너지학회 2008 신재생에너지 Vol.4 No.4
The possibility of whether the induced wind from a vehicle traveling on highway can be used in wind power generation has been verified through computational flow analysis. The bus which is presumed to accompany relatively strong and wide range of induced wind compared to passenger vehicles because of its wide frontal area has been set as the subject of research. In order to ensure the reliability of research, the flow analysis surrounding the bus on a flat road where median strip is not installed has been compared with a preceding research while the validity of grid system and interpretation method used in this research have been assured by a qualitative method. In case of the median strip type wind power generator system, because it has been verified that a strong streamwise wind speed (5 m/s) is derived from the contraction effect of flow passage between the bus and the median strip while maintaining a relatively consistent upwind wind speed (1.4 m/s) in vertical direction in the wake area after the bus passes by although the change of wind speed is intense, it was decided as having some possibility of wind power generation. In case of the traffic sign panel type wind power generator system installed at the upper top of highway, because the wind speed of 2 m/s level has been derived for a limited time only at a section equal to the length of the bus and a faint induced wind speed less than 0.5 m/s was shown at other regions, it was decided as having almost no possibility of wind power generation.