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LOW TEMPERATURE SYNTHESIS OF Fe-DOPED ZnO NANOROD BUNDLES IN AQUEOUS SOLUTION
FENGXIA GENG,HUI-MING CHENG,ZHIGANG ZHAO,HONGTAO CONG,JINBO BAI 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2006 NANO Vol.1 No.2
Pure and Fe-doped ZnO nanorod bundles were synthesized in aqueous solution at low temperature, in which inexpensive reagents such as Zn(NO3)2, NaOH and Fe(NO3)3 were used as precursors. The composition of the final product can be roughly tuned by the precursor ratio used. Energy dispersive X-ray spectroscopy confirms the successful incorporation of Fe element into ZnO nanorods, and X-ray diffraction reveals that ZnO nanorod bundles have a pure hexagonal wurtzite-phase structure. UV–vis spectroscopy show that the spectrum shifts to longer wavelength with increasing iron doping.
LOW TEMPERATURE SYNTHESIS OF Mg(OH)2 NANOTUBES IN AQUEOUS SOLUTIONS OF BLOCK COPOLYMER P123
HUI-MING CHENG,ZHIGANG ZHAO,FENGXIA GENG,HONGTAO CONG,JINBO BAI 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2006 NANO Vol.1 No.2
A simple aqueous solution-based block-polymer-assisted method was developed for the synthesis of Mg(OH)2 nanotubes using inexpensive starting materials (MgSO4 and NaOH) with significant advance of bringing down the average outer diameter to the regime below 10 nm. The synthesized nanotubes are found to possess a relatively high specific surface area up to 64 m2/g, which may suggest their potential value for use in the catalysis field. The Barrett–Joyner–Halenda pore-size distribution plot reveals a bimodal distribution centred at 3.4 and 17.3 nm, which may be from the tunnel cavity and the aggregated pores of Mg(OH)2 nanotubes, respectively. This method can be widely used to fabricate other inorganic 1D nanostructured materials and easily realized in industrial-scale synthesis.