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AAO Template를 이용한 Au/TiO<sub>2</sub> 나노섬유 제조 및 응용에 관한 연구
엄선미,박상선,김영덕,김용록,설용건,Eom, Seon-Mi,Park, Sang-Sun,Kim, Young-Deok,Kim, Yong-Rok,Shul, Yong-Gun 한국전기화학회 2009 한국전기화학회지 Vol.12 No.1
본 연구에서는 불순물이 포함된 Al 기판으로부터 두 단계의 양극산화 (anodization) 법에 의해 균일한 나노기공을 갖는 AAO(Anodic Aluminum Oxide)을 제조하였다. 생성된 AAO템플릿 위에 Deposition-Precipitation(DP)방법을 사용하여 수직으로 형성된 $TiO_2$ 나노섬유에 Au를 첨가시켜 2 wt.% $Au/TiO_2$ 나노섬유룰 제조하였다. 두 단계의 양극산화를 통해 규칙적으로 배열된 AAO 기공 형상과 기판 위에 수직으로 배향된 $TiO_2$ 나노섬유의 형상을 SEM을 통해 확인하였다. 또한 $Au/TiO_2$ 나노섬유의 특성은 XRD와 Raman 분석을 통하여 $TiO_2$의 아나타제(anatase)와 루타일(rutile) 결정구조와 $TiO_2$ 나노섬유에 담지된 Au의 존재를 확인하였다. 또한 일산화탄소(CO) 산화반응을 통해 AAO(Anodic Aluminum Oxide)기판 위에 형성된 $TiO_2$와 2 wt% $Au/TiO_2$ 나노섬유의 광촉매적 활성을 비교하였다. In this study, highly ordered AAO (Anodic Aluminum Oxide) with nanopores was prepared by commercial grade Al substrate containing 3.5 wt.% impurities through two step anodizing method. Nanopores of prepared AAO arrays were used as templates for preparing nanofiber. $TiO_2$ was deposited by using DP (deposition-precipitation) method into AAO pores to grow nanofiber. Au particles were loaded on this $TiO_2$ nanofiber which was grown vertically. Prepared 2 wt.% $Au/TiO_2$ nanofiber was characterized by XRD, SEM and Raman. The crystal structure was analyzed by the XRD. SEM was used to observe pore size and pore wall thickness. Photocatalytic activity of co-oxidation was compared with $TiO_2$ and $Au/TiO_2$ nanofiber on AAO arrays.
다중물리 유한요소해석에 의한 SiC 단결정의 용액성장 공정 설계
윤지영,이명현,서원선,설용건,정성민,Yoon, Ji-Young,Lee, Myung-Hyun,Seo, Won-Seon,Shul, Yong-Gun,Jeong, Seong-Min 한국결정성장학회 2016 한국결정성장학회지 Vol.26 No.1
용액성장법에 의한 SiC 단결정 성장은 Si 또는 Si-금속합금의 융액으로부터 SiC를 성장시키는 방법으로서, 통상의 상부종자 용액성장법(Top Seeded Solution Growth)에서는 Si 융액을 담는 흑연도가니로부터 C가 Si 융액에 용해되고 용해된 C이 상부에 위치한 종자결정으로 이동하여 종자결정상에 SiC 형태로 재결정화하는 단계를 거쳐 SiC의 단결정을 성장시키는 과정을 거치게 된다. SiC 용액성장에 있어서는 SiC의 단결정성장을 위하여 흑연도가니의 형상, 크기, 재질 및 상대적 위치 배열 등 온도제어와 유체흐름 제어를 위해 다양한 공정변수를 선정해야한다. 본 연구에서는 용액성장공정의 설계를 위해 상용의 유한요소해석 패키지인 COMSOL Multiphysics를 이용하여 전자기장해석, 열전달해석, 유체해석에 대한 다중물리해석모델을 구축하고 이 모델을 이용하여 결정성장공정을 설계하였다. 해석결과에 기초하여 2 inch off-axis 4H-SiC 단결정을 종자결정으로 적용하여 $1700^{\circ}C$에서 상부종자 용액성장법에 의하여 SiC 단결정을 성장시켰다. 광학현미경 및 고분해능 X선회절분석을 통해 결정성을 분석한 결과 해당 성장조건에서 양호한 품질의 단결정이 성장함을 확인하였다. 이로써 본 연구에서 구축된 다중물리해석모델이 SiC의 용액성장 공정설계에 유효함을 확인하였다. A top-seeded solution growth (TSSG) is a method of growing SiC single crystal from the Si melt dissolved the carbon. In this study, multiphysics modeling was conducted using COMSOL Multiphysics, a commercialized finite element analysis package, to get analytic results about electromagnetic analysis, heat transfer and fluid flow in the Si melt. Experimental results showed good agreements with simulation data, which supports the validity of the simulation model. Based on the understanding about solution growth of SiC and our set-up, crystal growth was conducted on off-axis 4H-SiC seed crystal in the temperature range of $1600{\sim}1800^{\circ}C$. The grown layer showed good crystal quality confirmed with optical microscopy and high resolution X-ray diffraction, which also demonstrates the effectiveness of the multiphysics model to find a process condition of solution growth of SiC single crystal.
공업화학 , 촉매 / 반응공학 : 알칼리이온이 치환된 제올라이트 상에서의 o-Xylene 의 알케닐화 반응
김전태(Jeon Tae Kim),조영상(Young Sang Cho),설용건(Yong Gun Shul),김영대(Young Dae Kim) 한국화학공학회 2001 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.39 No.3
The gas phase alkenylation of o-xylene with 1,3-butadiene was studied on the alkali cation exchanged zeolites X and Y. The alkenylation product, 5-(o-tolyl)-pentene, is a major precursor of 2,6-dimethylnaphthalene which is the raw material of polyethylene naphthalate (PEN). The relation between the basicity of the alkali canon exchanged zeolites and the alkenylation activity and selectivity was investigated. It was found by TPD analysis that there were two kinds of basic sites on the alkali canon exchanged zeolites: one was weak and the other was strong. The activity of alkenylation of o-xylene increased with the amount of the weak basic sites, while the selectivity of 5-(o-tolyl)-pentene enhanced with the amount of the strong basic sites on the catalysts.
MFI형 제올라이트 분리막을 이용한 에틸벤젠/파라자일렌 분리에 대한 연구
이기천 ( Gi Cheon Lee ),전유권 ( Yu Kwon Jeon ),주영환 ( Young Hwan Chu ),최성환 ( Seong Hwan Choi ),서영종 ( Young Jong Seo ),설용건 ( Yong Gun Shul ) 한국화학공학회 2013 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.51 No.4
Ethylbenzene (EB) which has a similar physical properties with p-xylene (pX) was separated from EB/pX mixture by using MFI-type zeolite (TS-1, ZSM-5, and Silicalite-1) coated membranes. The zeolites were synthesized by microwave method to reduce the synthesis time and uniformly formed zeolite particles were coated on the α-almina tubular support with a thickness of 3-4 μm. Separation factor and permeation flux of the synthesized zeolite coated membranes were measured to survey the best performance of ethylbenzene separation from different composition of EB/pX mixtures. When the EB/pX mixture of 5:5 molar ratio applied for the separation experiment, it represented the highest separation factor. We also have studied about the effect of the atomic composition of zeolites on the separation performance within the temperature range from 160 to 220℃. TS-1 showed the highest permeation flux of 1,666 mol/㎡*s*Pa and Silicate-1 showed the highest separation factor of 1.73 at 200℃ respectively.