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민병훈(Byong Hun Min) 한국에너지기후변화학회 2012 에너지기후변화학회지 Vol.7 No.2
The rational management of energy recovery over a wide range of temperature is possible with chemical heat pump using reversible solid-gas reaction. Because of the low heat transfer rate due to the gas phase, enhancement of heat transfer in the reactor bed is one of the most important subjects for developing gas-solid chemical heat pumps. In this study, the decane was used as liquid solvent to promote heat transfer in the chemical heat pump system utilizing CaCl₂-CH₃OH as working pair. Because in the several cycle, pseudo equilibrium hysteresis behavior was not observed in the synthesis and decomposition reactions, the suspension phase with solvent in the reactors has shown that it is possible to achieve continuous operation of solid-gas chemical heat pump. The equilibrium curve for pressuretemperature was expressed in the form of vant Hoff equation. The simulated calculation of coefficient of performance was performed over the operating conditions.
김종문(Jong-Moon Kim),정찬교(Chan-Kyo Chung),민병훈(Byong-Hun Min) 한국청정기술학회 2013 청정기술 Vol.19 No.4
본 연구에서는 국내에서 대표적으로 버려지는 폐벌목 중 잣나무에서 만든 활성탄을 이용하여 벤젠에 대한 정지(static)흡착실험을 수행하였다. 7.999 kPa에 이르는 압력 범위 내에서 온도 조건을 변화시켜 가며 303.15, 318.15, 333.15 K에서 흡착실험을 진행하였다. 등온흡착곡선은 Langmuir 등온흡착식, Freundlich 등온흡착식, Toth 등온흡착식을 적용하여 비교하였다. 벤젠의 흡착량(q)을 측정한 결과 Langmuir 등온흡착식과 Toth 등온흡착식으로 적용한 등온흡착곡선의 정확도가 높은 것으로 나타났다. 그리고 Langmuir 등온흡착식의 qmax 값을 이용하여 흡착제의 흡착량을 비교하였다. 또한, 폐벌목 활성탄과 상용활성탄의 세공 발달 여부를 비교하기 위해 주사전자현미경(scanning electron microscopy, SEM) 사진을 관찰하였다. SEM 사진 관찰 결과, 폐벌목 활성탄이 국내?외 상용활성탄(DARCO A.C., SPG-100 A.C.)에 비해 세공발달 정도가 우수하며, 벤젠흡착량(q)이 높은 것을 확인할 수 있었다. 본 연구 결과를 통해 폐벌목 활성탄의 상용화 가능성을 검증할 수 있었다. In this study, experiments on the static adsorption of benzene were carried out using activated carbon made from Pinus koraiensis which is normally discarded waste timber in South Korea. The experiment were performed at 303.15 K, 318.15 K and 333.15 K under the pressure up to 7.999 kPa. Isothermal adsorption curves were obtained using Langmuir isotherm, Freundlich isotherm and Toth isotherm for comparison. Based on the fitting, the adsorption quantity of Benzene (q), the isothermal adsorption curves obtained from Langmuir isotherm and Toth isotherm showed the higher accuracy. Although there was little difference in accuracy between result from Langmuir isotherm and that from Toth isotherm, the adsorption quantity of Benzene (q) was expressed in terms of Langmuir isotherm because less parameters were required for Langmuir isotherm than for Toth isotherm. Moreover SEM images of the activated carbon from Pinus koraiensis and the commercial activated carbon were taken to observe the pore size development. The results showed that the perforation development of activated carbon from Pinus koraiensis (waste timber) was better than that of commercial activated carbon (DARCO A.C., SPG-100 A.C.). Adsorption quantity of benzene on activated carbon from Pinus koraiensis was confirmed to be higher than that on commercial activated carbon. Therefore, we may conclude that it is feasible to commercialize the process to manufacturing activated carbon from waste timber.
Poly(hexamethylene carbonate) glycol/Poly(oxytetramethylene) glycol 혼합 폴리올을 도입한 수분산성 폴리우레탄의 제조와 물성
조철희 ( Cheol Hee Cho ),서희동 ( Hee Dong Seo ),민병훈 ( Byong Hun Min ),조항규 ( Hang Kyu Cho ),노시태 ( Si Tae Noh ),최형기 ( Heong Gi Choi ),조영호 ( Young Ho Cho ),김정호 ( Jeong Ho Kim ) 한국공업화학회 2002 공업화학 Vol.13 No.8
Poly[hexamethylene carbonate] glycol (PHMCG)과 poly[oxytetramethylene] glycol (PTMG)을 각각 카보네이트 폴리올 및 에테르 타입의 폴리올로 사용하고 여기에 잠재적 음이온기인 dimethylol propionic acid (DMPA)와 이소시아네이트 화합물인 isophorone diisocyanate (IPDI)를 첨가하여 음이온성 폴리우레탄 분산체 (PUD)를 제조하였다. 두가지 형태의 폴리올을 각각 단독으로 사용할 때와 혼합하여 사용할 때 폴리올의 조성 및 종류가 PUD의 유화 입경과 건조 필름의 기계적, 열적 물성에 미치는 영향 등에 대해 검토하였는데 혼합 폴리올 적용시 PTMG 함량이 증가할수록 PUD의 유화 입경이 점차적으로 증가하는 경향을 보였고, 인장 강도는 완만한 가소를 나타나다가 증가하였다. 이는 두 폴리올간의 상용성이 적기 때문에 나타나는 결과로 해석되며, 이러한 비상용성은 DSC 분석을 통하여 확인할 수 있었다. Using poly [hexamethylene carbonate] glycol (PHMCG) and poly[oxytetramethylene] glycol (PTMG) as the carbonate type and ether type polyols, respectively, and by adding isophorone diisocyanate (IPDI) and dimethylol propionic acid (DMPA), polyurethane dispersions (PUD) were prepared. The effect of type and composition of polyols on the particle size of PUD and on the mechanical and thermal properties of PUD cast films were investigated. As the PTMG contents in the mixed polyols increased the particle size asymptotically increased, while tensile strength showed a slight decrease followed by a slight increase. This was due to the incompatibility of two polyols, which was confirmed by DSC analysis.