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김문집,전기배 순천향대학교 기초과학연구소 2008 순천향자연과학연구 논문집 Vol.14 No.2
The structure of C_(13)H_(12)N₂OCu½Cl has been determined by X-ray diffraction methods. The crystal system is monoclinic, space group P1^( ̄), unit cell constants, a=8.705(3)Å, b=9.818(3)Å, c=9.822(4)Å, α=111.28(2)˚, β=96.75(5)˚, γ=90.25(4)˚, V=775.8(5)ų, T= 293(2)K, Z=2, D_(C) = 1.402Mgm^(-)³. The intensity data were collected on an Enraf-Nonius CAD-4 Diffractometer with graphite monochromated Cu Ka radiation (λ=1.54184Å). The molecular structure was solved by direct methods and refined by full-matrix least squares to a final R = 5.76% for 2684 unique observed F_(0) > 4σ(F_(0)) reflections and 188 parameters.
김문집,전기배 순천향대학교 기초과학연구소 2007 순천향자연과학연구 논문집 Vol.13 No.2
The structure of C_(20)_H_(22)N₂O₂MnCl has been determined by X-ray diffractiun methods. The crystal system is monoclinic, space group P2₁/α, unit cell constants, α = 14.8967(27) Å, b= 18.6446 (36)Å, c = 6.8836(7)Å, β = 92.32(2)˚, V = 1910.30(15) ų, T=293(2)K, Z=4, D_(c) = 1.435Mgm^(-3). The intensity data were collected on an Enraf-Nonius CAD-4 Diffractometer with graphite monochromated Mo Kα radiation(λ = 0.71073 Å). The molecular structure was sulved by direct methods and refined by full-matrix least squares to a final R=6.73% for 1670 unique observed F_(0)>4σ(F_(0)) reflections and 239 parameters.
김문집,전기배 순천향대학교 기초과학연구소 2007 순천향자연과학연구 논문집 Vol.13 No.2
The structure of C_(15)H_(9)O₂NCl₂ has been determined by X-ray diffraction methods. The crystal system is monoclinic, space group P2₁/α, unit cell constants, α = 14.603(l)Å, b = 6.162(1)Å, c = 15.685(1)Å, β = 112.233(6)˚, V = 1306.45(17)ų, T = 293(2)K, Z=4, D_(c)= 1.556Mgm^(-3). The intensity data were collected on an Enraf-Nonius CAD-4 Diffractometer with graphite monochromated Cц Kα radiation (λ = 1.54184Å). The molecular structure was solved by direct methods and refined by full-matrix least squares tu a final R = 7.26% fur 1405 unique observed F_(0)> 4σ(F_(0)) reflections and 181 parameters.