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한반도 남부지역에서 산출되는 카올린광물의 고온영역에서의 광물학적 특성 연구
이수정,문희수,Lee, Su-Jeong,Moon, Hi-Soo 대한자원환경지질학회 1996 자원환경지질 Vol.29 No.3
Dehydroxylation and mullitization of primary and secondary kaolins were investigated in order to compare and understand the differences in thermal behaviours by DTA and TG up to $1,100^{\circ}C$. Chemical analyses and EPMA of the samples revealed nearly ideal unit-cell formulae of kaolins. The weight losses of dickite and halloysite are 14% and 12.5% on the average, respectively. The activation energies of dehydroxylation of kaolin minerals were calculated according to Kissinger's approach which uses various heating rates in DTA to estimate the activation energy of thermal reactions. The activation energies of dehydroxylation of halloysites from Daemoung and Buksam mines are about $163kJmor^{-1}$ (white), $168kJmor^{-1}$ (pink), and $176kJmor^{-1}$ respectively. The activation energies of dickites collected from Sungsan and Ogmae mines are about $166kJmor^{-1}$ and $387kJmor^{-1}$. The asymmetric shape of endothermic peak in DTA, the relative intensities of OH-stretching bands in FTIR spectroscopy and the existence of residual XRD peaks of the samples which were heated at $550^{\circ}C$ for 2 hours indicate that Sungsan dickite may be more disordered than Ogmae dickite. The new phase formed in thermally treated samples in the range of $900^{\circ}C$ to $1,100^{\circ}C$ was identified as mullite by XRD on the basis of disappearing of the characteristic peaks of kaolins and increasing of amorphous background upon heat treatment. On further heating, loss of more water from dehydroxylate resulted in the formation of mullite and the characteristic X-ray diffraction patterns of mullite began to appear at about $900{\sim}1,000^{\circ}C$ in kaolins.
Texture Electron Diffraction Pattern에 의한 결정구조 해석
이수정,주형태,김윤중,문희수,Lee, Su-Jeong,Jou, Hyeong-Tae,Kim, Youn-Joong,Moon, Hi-Soo 한국현미경학회 2002 Applied microscopy Vol.32 No.3
Texture electron diffraction pattern을 이용한 결정구조 해석 이론은 러시아어로 씌여졌거나, 영문판 저서의 일부에 간단히 소개 되어있어 이해에 어려움이 있다. 이들의 이론은 벡터의 이론과 관련된 여러 관계식을 이용해서 설명될 수 있으며, 이로서 몇 개의 식에 포함된 오류를 수정하였다. The works of texture electron diffraction patterns for crystal structure analysis are written in Russian or introduced briefly in books written in English, which makes it difficult to be understood. In addition to working out the equations, vector theory corrects some errors included in the established formulas for texture electron diffraction patterns.